Collection of scientific works Nanosystems, nanomaterials, nanotechnologies
Year 2026 Volume 24, Issue 2
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A. V. LYSYTSYA1, V. O. MYSLINCHUK1, M. V. MOROZ2, B. D. NECHYPORUK1, N. S. PAVLOVA1, B. P. RUDYK2, and B. A. TATARYN3

1Rivne State University of Humanities, 31 Plastova Str., UA-33000 Rivne, Ukraine
2National University of Water and Environmental Engineering, 11, Soborna Str., UA-33000 Rivne, Ukraine
3Lesya Ukrainka Volyn National University, 13, Voli Ave., UA-43025 Lutsk, Ukraine

Study of the Structure of Cadmium Sulphide Nanocrystals

533–547 (2026)

PACS numbers: 61.05.cp, 61.46.Hk, 61.66.Fn, 81.07.Bc, 81.10.Jt, 82.80.Fk

Received 13 February, 2026

In this work, cadmium-sulphide nanocrystals are studied, which are obtained by the electrolytic method using cadmium electrodes and an aqueous solution of sodium thiosulphate as an electrolyte. X-ray structural studies are carried out, and the composition of the obtained samples is determined. The parameters of the crystal lattice are established, and the sizes of the nanocrystals are calculated using the Debye–Scherrer formula, the Williamson–Hall method, and the size-deformation method. As revealed, the obtained cadmium sulphide nanocrystals contain two phases: sphalerite and wurtzite; the volume content of these two phases is also determined.

KEY WORDS: nanocrystals, cadmium sulphide, electrolytic method for fabrication of nanocrystals, x-ray diffraction analysis, crystal-lattice parameter, nanoparticle sizes, Debye–Scherrer formula, Williamson–Hall method, size-deformation method

DOI: https://doi.org/10.15407/nnn.24.02.0533

Citation:
A. V. Lysytsya, V. O. Myslinchuk, M. V. Moroz, B. D. Nechyporuk, N. S. Pavlova, B. P. Rudyk, and B. A. Tataryn, Study of the Structure of Cadmium Sulphide Nanocrystals, Nanosistemi, Nanomateriali, Nanotehnologii, 24, No. 2: 533–547 (2026); https://doi.org/10.15407/nnn.24.02.0533
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